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The continued development of metal additive manufacturing (AM) has expanded the engineering metallic alloys for which these processes may be applied, including beta-titanium alloys with desirable strength-to-density ratios. To understand the response of beta-titanium alloys to AM processing, solidification and microstructure evolution needs to be investigated. In particular, thermal gradients (Gs) and solidification velocities (Vs) experienced during AM are needed to link processing to microstructure development, including the columnar-to-equiaxed transition (CET). In this work, in situ synchrotron X-ray radiography of the beta-titanium alloy Ti-10V-2Fe-3Al (wt.%) (Ti-1023) during simulated laser-powder bed fusion (L-PBF) was performed at the Advanced Photon Source at Argonne National Laboratory, allowing for direct determination of Vs. Two different computational modeling tools, SYSWELD and FLOW-3D, were utilized to investigate the solidification conditions of spot and raster melt scenarios. The predicted Vs obtained from both pieces of computational software exhibited good agreement with those obtained from in situ synchrotron X-ray radiography measurements. The model that accounted for fluid flow also showed the ability to predict trends unobservable in the in situ synchrotron X-ray radiography, but are known to occur during rapid solidification. A CET model for Ti-1023 was also developed using the Kurz–Giovanola–Trivedi model, which allowed modeled Gs and Vs to be compared in the context of predicted grain morphologies. Both pieces of software were in agreement for morphology predictions of spot-melts, but drastically differed for raster predictions. The discrepancy is attributable to the difference in accounting for fluid flow, resulting in magnitude-different values of Gs for similar Vs. 

Abstract The individual effects of strain rate and temperature on the strain hardening rate of a quenched and partitioned steel have been examined. During quasistatic tests, resistive heating was used to simulate the deformation-induced heating that occurs during high-strain-rate deformation, while the deformation-induced martensitic transformation was tracked by a combination of x-ray and electron backscatter diffraction. Unique work hardening rates under various thermal–mechanical conditions are discussed, based on the balance between the concurrent dislocation slip and transformation-induced plasticity deformation mechanisms. The diffraction and strain hardening data suggest that the imposed strain rate and temperature exhibited dissonant influences on the martensitic phase transformation. Increasing the strain rate appeared to enhance the martensitic transformation, while increasing the temperature suppressed the martensitic transformation. 

Quenching and partitioning (Q&P) processing of third-generation advanced high strength steels generates multiphase microstructures containing metastable retained austenite. Deformation-induced martensitic transformation of retained austenite improves strength and ductility by increasing instantaneous strain hardening rates. This paper explores the influence of martensitic transformation and strain hardening on tensile performance. Tensile tests were performed on steels with nominally similar compositions and microstructures (11.3 to 12.6 vol. pct retained austenite and 16.7 to 23.4 vol. pct ferrite) at 980 and 1180 MPa ultimate tensile strength levels. For each steel, tensile performance was generally consistent along different orientations in the sheet relative to the rolling direction, but a greater amount of austenite transformation occurred during uniform elongation along the rolling direction. Neither the amount of retained austenite prior to straining nor the total amount of retained austenite transformed during straining could be directly correlated to tensile performance. It is proposed that stability of retained austenite, rather than austenite volume fraction, greatly influences strain hardening rate, and thus controls strength and ductility. If true, this suggests that tailoring austenite stability is critical for optimizing the forming response and crash performance of quenched and partitioned grades.